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1、ASTM_D3359-02胶带试验测定粘合性的方法Designation:D3359-02名称：D335902StandardTestMethodsforMeasuringAdhesionbyTapeTest1胶带试验测定粘合性的方法ThisstandardisissuedunderthefixeddesignationD3359;thenumberimmediatelyfollowingthedesignationindicatestheyearoforiginaladoptionor,inthecaseofrevision,theyearoflastrevision.Anumberinpa
2、renthesesindicatestheyearoflastreapproval.Asuperscriptepsilon(e)indicatesaneditorialchangesincethelastrevisionorreapproval.这个标准是D3359确定了以后发行的。数字代表名称最初通过的时间，或者修订情况，和最新版本。括号内的数字代表最新重新审批时间。上标代表最新版本的变化或重新审批。ThisstandardhasbeenapprovedforusebyagenciesoftheDepartmentofDefense.该标准已经被国防机构部门批准使用。1. Scope范围1.
3、1 Thesetestmethodscoverproceduresforassessingtheadhesionofcoatingfilmstometallicsubstratesbyapplyingandremovingpressure-sensitivetapeovercutsmadeinthefilm.这些试验方法覆盖了对金属涂层片附着力的评估。附着性通过在涂层切口处施加和去除透明压敏胶带来评估。1.2 TestMethodAisprimarilyintendedforuseatjobsiteswhileTestMethodBismoresuitableforuseinthelabora
4、tory.Also,TestMethodBisnotconsideredsuitableforfilmsthickerthan5mils(125m).试验方法A主要用于工作场所，而试验方法B更适用与实验室。试验方法B不适宜在涂层厚度大于125微米时使用。NOTE1Subjecttoagreementbetweenthepurchaserandtheseller,TestMethodBcanbeusedforthickerfilmsifwiderspacedcutsareemployed.在买方和卖方之间的协议，如果允许更宽的切口，方法B可以用在更厚的涂层上。1.3 Thesetestmetho
5、dsareusedtoestablishwhethertheadhesionofacoatingtoasubstrateisatagenerallyadequatelevel.Theydonotdistinguishbetweenhigherlevelsofadhesionforwhichmoresophisticatedmethodsofmeasurementarerequired.这些试验方法被用来确定涂层对底材是否有足够的附着力。不区分层次,以服从需要更先进的测量方法。NOTE2Itshouldberecognizedthatdifferencesinadherabilityofthec
6、oatingsurfacecanaffecttheresultsobtainedwithcoatingshavingthesameinherentadhesion.备注2：应该承认，涂层表面附着力的差异影响涂相同附着性的涂层得到的结果。1.4 Inmulticoatsystemsadhesionfailuremayoccurbetweencoatssothattheadhesionofthecoatingsystemtothesubstrateisnotdetermined.多层系统的失效发生涂层之间，以致使涂层与基层之间的粘附性无法确定。1.5 ThevaluesstatedinSIunit
7、saretoberegardedasthestandard.Thevaluesgiveninparenthesesareforinformationonly.SlD单位价值被视为标准，括号内的价值是仅供参考.1.6 Thisstandarddoesnotpurporttoaddressthesafetyconcerns,ifany,associatedwithitsuse.Itistheresponsibilityoftheuserofthisstandardtoestablishappropriatesafetyandhealthpracticesanddeterminetheapplica
8、bilityofregulatorylimitationspriortouse.这个标准不打算讨论安全问题,如果有的话,再加上使用.用户有责任建立适当的安全标准和卫生管理办法和确定适用前使用限制.2. ReferencedDocuments参考文件2.1 ASTMStandards:美国材料与试验协会标准D609PracticeforPreparationofCold-RolledSteelPanelsforTestingPaint,Varnish,ConversionCoalings,andRelatedCoatingProducts2D609实际编写冷轧钢板测试油漆、油光漆、转换材料、涂料
9、及相关产品2D823PracticesforProducingFilmsofUniformThicknessofPaint,Varnish,andRelatedProductsonTestPanels2D823方法制作影片制服油漆厚度、油光漆及相关产品测试板2D1000TestMethodForPressure-SensitiveAdhesive-CoatedTiipesUsedforElectricalandElectronicApplications3DIOoO测试方法压力敏感粘合剂镀磁带用于电器及电子应用3D1730PracticesforPreparationofAluminumand
10、Aluminum-AlloySurfacesforPainting4D1730方法编制铝和铝的合金表面油漆4D2092GuideforPreparationofZinc-Coated(Galvanized)SteelSurfacesforPainting5D2092锌编制指南在钢表面(镀锌)。D2370TestMethodforTensilePropertiesofOrganicCoatings2D2370测试方法为有机涂层2的拉力特性。D3330TestMethodforPeelAdhesionofPressure-SensitiveTape6D3330测试方法：压敏胶带6D3924Spec
11、ificationforStandardEnvironmentforConditioningandTestingPaint,Vamish,Lacquer,andRelatedMaterials2D3924标准规格的环境试验条件和油漆,油光漆、漆器、副产品2D4060TestMethodforAbrasionResistanceofOrganicCoalingsbytheTaberAbraser2D4060测试方法：用泰伯耐磨性测定仪测定有机涂层的抗磨损。3. SummaryofTestMethods试验方法摘要3.1 TestMethodA-AnX-cutismadethroughthefil
12、mtothesubstrate,pressuresensitivetapeisappliedoverthecutandthenremoved,andadhesionisassessedqualitativelyonthe0to5scale.试验方法A：一个X槽贯通涂层和底材，在切口上放置和移除胶带，粘附力按照0-5质量等级进行评估。3.2 TestMethodBAlatticepatternwitheithersixorelevencutsineachdirectionismadeinthefilmtothesubstrate,pressure-sensitivetapeisappliedov
13、erthelatticeandthenremoved,andadhesionisevaluatedbycomparisonwithdescriptionsandillustrations.试验方法B：在涂层与底材之间切割六或十一晶格形态的截割切片，在晶格之间施加和移动胶带，粘附力通过图表描述对比来做评估。4. SignificanceandUse意义和用途1 .1Ifacoatingistofulfillitsfunctionofprotectingordecoratingasubstrate,itmustadheretoitfortheexpectedservicelife.Becauset
14、hesubstrateanditssurfacepreparation(orlackofit)haveadrasticeffectontheadhesionofcoatings,amethodtoevaluateadhesionofacoatingtodifferentsubstratesorsurfacetreatments,orofdifferentcoatingstothesamesubstrateandtreatment,isofconsiderableusefulnessintheindustry.如果涂层是满足保护或装饰底材，必须要达到预期的服务寿命。因为底材和其表面处理(或缺乏)
15、对涂层的附着性有强烈的影响，评价方法加入了不同涂层表面处理、沼气、各种材料的原子相同的待遇,是相当有用的产业。2 ThesetestmethodsareunderthejurisdictionofASTMCommitteeDOlonPaintandRelatedCoatings,Materials,andApplicationsandarethedirectresponsibilityofSubcommitteeDO1.23onPhysicalPropertiesofAppliedPaintFilms.测试方法在美国材料与试验协会DOl关于油漆和有关涂层、材料、应用软件和关于油漆涂层的物理性能
16、D01.23的权限下进行的。CurrenteditionapprovedAug.10,2002.PublishedOctober2002.OriginallypublishedasD3359-74.LastpreviouseditionD3359-97.3 AnnualBookofASTMStandards,Vol06.01.4 AnnualBookofASTMStandards,Vol10.01.5 AnnualBookofASTMStandards,Vol02.05.6 AnnualBookofASTMStandards,Vol06.02.6AnnualBookofASTMStandard
17、s,Vol15.09.最新版本在2002年8月10号被认可。2002年10月出版。最初出版是D3359-74,上一个版本是D3359-97。CopyrightASTMInternational,100BarrHarborDrive,POBoxC700,WestConshohocken,PA19428-2959,UnitedStates.CopyrightASTMInternationalReproducedbyIHSunderlicensewithASTMLicensee=CiaimIerchyrsleraccount/5957216001NotforResale,12/09/200500:3
18、4:54MSTNoreproductionornetworkingpermittedwithoutlicensefromIHS7 .2Thelimitationsofalladhesionmethodsandthespecificlimitationofthistestmethodtolowerlevelsofadhesion(see1.3)shouldberecognizedbeforeusingit.Theintra-andinter-laboratoryprecisionofthistestmethodissimilartootherwidely-acceptedtestsforcoat
19、edsubstrates（forexample,TestMethodD2370andTestMethodD4060）,butthisispartlytheresultofitbeinginsensitivetoallbutlargedifferencesinadhesion.Thelimitedscaleof0to5wasselecteddeliberatelytoavoidafalseimpressionofbeingsensitive.使用前应承认，所有附着力方法的局限性和这个试验方法对下一级附着力（见7.3） 的特殊的限制。内部和跨实验室精密这种测试方法类似其他广泛接受测试动听基质（如测
20、试方法D2370及测试方法D4060）,但大部分结果是不敏感的，除了附着力的不同。在有限的范围内选择55刻意避免在敏感的假象。TESTMETHODA-X-CUTTAPETEST试验方法A：X截割（X切片）5. ApparatusandMaterials仪器和材料5.1 CuttingTool-Sharprazorblade,scalpel,knifeorothercuttingdevices.Itisofparticularimportancethatthecuttingedgesbeingoodcondition.切削刀具：一一整刀片、手术刀、刀或者其他切削设备。5.2 CuttingGui
21、de-Steelorotherhardmetalstraightedgetoensurestraightcuts.引导切割一一钢的或其他金属画直线用尺来保证直线切削。5.3 Tape25-mm（1.0-in.）widesemitransparentpressuresensitivetape7withanadhesionstrengthagreeduponbythesupplierandtheuserisneeded.Becauseofthevariabilityinadhesionstrengthfrombatch-to-batchandwithtime,itisessentialthatta
22、pefromthesamebatchbeusedwhentestsaretoberunindifferentlaboratories.Ifthisisnotpossiblethetestmethodshouldbeusedonlyforrankingaseriesoftestcoatings.胶带一一25mm宽的半透明的透明压敏胶粘带和被供应商和用户同意的粘合力是需要的。因为粘合力是随着时间和批次变化的，重要的是当试验在不同的实验室进行时使用的带要是同一批次的。如果无法做到这一点，测试方法应仅用于一系列测试涂层排名。5.4 RubberEraser,ontheendofapencil.橡胶橡皮
23、5.5 Illumination-Alightsourceishelpfulindeterminingwhetherthecutshavebeenmadethroughthefilmtothesubstrate.照明一一当在切片和基体之间开有切口时，光源是有很有帮助的。6. TestSpecimens试样6.1 Whenthistestmethodisusedinthefield,thespecimenisthecoatedstructureorarticleonwhichtheadhesionistobeevaluated.当这个试验方法在这个领域使用时，试样的结构或物品上的粘附力都将要被评
24、估。6.2 Forlaboratoryuseapplythematerialstobetestedtopanelsofthecompositionandsurfaceconditionsonwhichitisdesiredtodeterminetheadhesion.实验室使用的申请材料进行试验,以面板的成份的和表面状况的需要来确定附着力。NOTE3ApplicabletestpaneldescriptionandsurfacepreparationmethodsaregiveninPracticeD609andPracticesD1730andD2092.备注3：可适用的测试板的描述和表面准
25、备方法见D609和D1730、D2092。NOTE4CoatingsshouldbeappliedinaccordancewithPracticeD823,orasagreeduponbetweenthepurchaserandtheseller.备注4：一涂层的应用按照D823,或者买方和卖方之间达成协议。NOTE5-Ifdesiredorspecified,thecoatedtestpanelsmaybesubjectedtoapreliminaryexposuresuchaswaterimmersion,saltspray,orhighhumiditybeforeconductingth
26、etapetest.Theconditionsandtimeofexposurewillbegovernedbyultimatecoatinguseorshallbeagreeduponbetweenthepurchaserandseller.备注4：一规定，涂层测试板在试验前最初应浸在水中，盐雾或高湿度中。浸泡的时间和条件应由最终用涂层决定或者买方和卖方之间达成协议。7. Procedure程序7.1 Selectanareafreeofblemishesandminorsurfaceimperfections.Fortestsinthefield,ensurethatthesurfacei
27、scleananddry.Extremesintemperatureorrelativehumiditymayaffecttheadhesionofthetapeorthecoating.选有瑕疵和表面缺陷的区域，在这个区域中做试验，确保表面是干净的和干燥的。极端的温度和相对湿度可能影响粘贴带或涂层。7.1.1 Forspecimenswhichhavebeenimmersed:Afterimmersion,cleanandwipethesurfacewithanappropriatesolventwhichwillnotharmtheintegrityofthecoating.Thendry
28、orpreparethesurface,orboth,asagreeduponbetweenthepurchaserandtheseller.对于被浸泡的样件，浸泡完以后用适当的溶剂(不能破坏涂层的完整性)擦净表面。然后准备或表面干燥,或在买方和卖方之间双方达成的协议,。7.2 Maketwocutsinthefilmeachabout40mm(1.5in.)longthatintersectneartheirmiddlewithasmallerangleofbetween30and45o.Whenmakingtheincisions,usethestraightedgeandcutthrou
29、ghthecoatingtothesubstrateinonesteadymotion.在涂层上切2个切口，每个40mm长，两切口在中间位置交叉成30-45。夹角。当切割切口时，用直线尺在涂层与底材之间做恒稳运动。7.3 Inspecttheincisionsforreflectionoflightfromthemetalsubstratetoestablishthatthecoatingfilmhasbeenpenetrated.IfthesubstratehasnotbeenreachedmakeanotherXinadifferentlocation.Donotattempttodeep
30、enapreviouscutasthismayaffectadhesionalongtheincision.检查切口处，从金属表面的反射光来确定涂层已经被穿透。如果底材没有达到，在不同位置再用X槽。不要试图加深以前切口的深度，这样可能影响切口处的附着性。7.4 Removetwocompletelapsofthepressure-sensitivetapefromtherollanddiscard.Removeanadditionallengthatasteady(thatis,notjerked)rateandcutapieceabout75mm(3in.)long.移动两个完全重叠的压敏粘
31、胶带。按均匀的速度拉出一段胶带，除去最前面的一段，然后剪下长约75mm胶带。7.5 Placethecenterofthetapeattheintersectionofthecutswiththetaperunninginthesamedirectionasthesmallerangles.Smooththetapeintoplacebyfingerintheareaoftheincisionsandthenrubfirmlywiththeeraserontheendofapencil.Thecolorunderthetransparenttapeisausefulindicationofwh
32、engoodcontacthasbeenmade.把胶带的中心放在网格上方，用手指把胶带在网格区上方的部位压平，为了保证胶带与涂层接触良好，用橡皮用力摩擦胶带。透过胶带看到涂层颜色全面接触是有效的显示。7.6 Within9030sofapplication,removethetapebyseizingthefreeendandpullingitoffrapidly(notjerked)backuponitselfatasclosetoanangleof180oaspossible.在贴上胶带9030秒时间内，拿住胶带悬空的一端，并在尽可能接近180度，快速地（不是颠簸的）撕离胶带。7.7 I
33、nspecttheX-cutareaforremovalofcoatingfromthesubstrateorpreviouscoatingandratetheadhesioninaccordancewiththefollowingscale:检查X切口面积减少拆除或涂层的基材上涂层和粘贴率按照下列范围：5ANopeelingorremoval,没有脱皮或移动4ATracepeelingorremovalalongincisionsorattheirintersection,在交叉点追踪或随着切口移动3AJaggedremovalalongincisionsupto1.6mm(1/16in.)
34、oneitherside,在切口的任意一侧移动1.6mm2AJaggedremovalalongmostofincisionsupto3.2mm(1/8in.)oneitherside,沿着大部分切口的任一侧锯齿状移动3.2mm1ARemovalfrommostoftheareaoftheXunderthetape,在胶带下面大部分X区域移动。andOARemovalbeyondtheareaoftheX.移动超出X区域。7.8 Repeatthetestintwootherlocationsoneachtestpanel.Forlargestructuresmakesufficienttes
35、tstoensurethattheadhesionevaluationisrepresentativeofthewholesurface.在另外两个地点重复测试每个测试小组。大型结构试验充分保证了粘合力评估代表整个表面。7.9 Aftermakingseveralcutsexaminethecuttingedgeand,ifnecessary,removeanyflatspotsorwire-edgebyabradinglightlyonafineoilstonebeforeusingagain.Discardcuttingtoolsthatdevelopnicksorotherdefects
36、thattearthefilm.切割了几个切口以后，检查切口边，如果需要，去除尖角(使用以前用油石去除)如果刀具损伤了涂层表面或刀具有缺口，丢弃刀具。Report报告8.1 Reportthenumberoftests,theirmeanandrange,andforcoatingsystems,wherethefailureoccurredthatis,betweenfirstcoatandsubstrate,betweenfirstandsecondcoat,etc.汇报试验的数量，平均和范围，对于涂层系统，失效发生在哪里，发生在第一个涂层和基体之间，还是在第一与第二涂层之间。8.2 Fo
37、rfieldtestsreportthestructureorarticletested,thelocationandtheenvironmentalconditionsatthetimeoftesting.报告测试的组织或项目，和试验时的环境情况。8.3 Fortestpanelsreportthesubstrateemployed,thetypeofcoating,themethodofcure,andtheenvironmentalconditionsatthetimeoftesting.测试板报告所用的底材，涂层的类型，治愈的方法，和试验时的环境情况。8.4 Iftheadhesion
38、strengthofthetapehasbeendeterminedinaccordancewithTestMethodsDIOOOorD3330,reporttheresultswiththeadhesionrating(s).Iftheadhesionstrengthofthetapehasnotbeendetermined,reportthespecifictapeusedanditsmanufacturer.如果胶带的附着力符合Dl(X)O或者D3330,记录附着力级别的结果。如果胶带附着力的大小没有确定，记录使用胶带的生产厂家和使用的型号。8.5 Pcrmacel99,manufac
39、turedbyPermacel,NewBrunswick,NJ08903,andavailablefromvariousPermaceltapedistributors,isreportedtobesuitableforthispurpose.Themanufacturerofthistapeandthemanufacturerofthetapeusedintheinterlaboratorystudy(seeRR:DOl-1008),haveadvisedthissubcommitteethatthepropertiesofthesetapeswerechanged.Usersofitsho
40、uld,therefore,checkwhethercurrentmaterialgivescomparableresultstoprevioussuppliedmaterial.CopyrightASTMInternationalReproducedbyIHSunderlicensewithASTMLicensee=Ciaimlerchyrsleraccount/5957216001NotforResale,12/09/200500:34:54MSTNoreproductionornetworkingpermittedwithoutlicensefromIHS未经IHS允许，不允许复制或网络
41、传播。8.6 Ifthetestisperformedafterimmersion,reportimmersionconditionsandmethodofsamplepreparation.如果试验在浸泡以后再进行，记录浸泡的条件和试样准备方法。9.Precision and Bias 8精度和偏差1.1 Inaninterlaboratorystudyofthistestmethodinwhichoperatorsinsixlaboratoriesmadeoneadhesionmeasurementonthreepanelseachofthreecoatingscoveringawider
42、angeofadhesion,theWithin-Iaboratoriesstandarddeviationwasfoundtobe0.33andthebetween-laboratories0.44.Basedonthesestandarddeviations,thefollowingcriteriashouldbeusedforjudgingtheacceptabilityofresultsatthe95%confidencelevel:在多个实验室进行的测试方法。操作者在6个实验室的3个平板上的涂层上覆盖一系列附着力，做同一个附着力测试。在同一个实验室的标准偏差为0.33,在不同实验室发
43、现偏差为0.44.以这些标准偏差为基础，以下标准应该用来确定结果的可行性有95%的可信度。1.1.1 RepeatabilityProvidedadhesionisuniformoveralargesurface,resultsobtainedbythesameoperatorshouldbeconsideredsuspectiftheydifferbymorethan1ratingunitfortwomeasurements.重复性：假定在一个大表面的附着力是一致的，同一个操作者两次测量得到的结果差异超过一个单位等级，那麽将被认为是不可信的。1.1.2 Reproducibility-Two
44、results,eachthemeanoftriplicates,obtainedbydifferentoperatorsshouldbeconsideredsuspectiftheydifferbymorethan1.5ratingunits.再现性：取每个操作者3次测量的均值，如果得到的两个结果超过1.5个单位等级，那麽将被认为是不可信的。1.2 Biascannotbeestablishedforthesetestmethods.用这些测试方法不能确定偏差。TESTMETHODBCROSSCUTTAPETEST测试方法B：交叉切口胶带测试10. ApparatusandMaterials
45、器具和材料10.1 CuttingTool9一Sharprazorblade,scalpel,knifeorothercuttingdevicehavingacuttingedgeanglebetween15and30othatwillmakeeitherasinglecutorseveralcutsatonce.Itisofparticularimportancethatthecuttingedgeoredgesbeingoodcondition.切割刀具：一一锋利的刀刃、手术刀、刀或者其他切削设备的切削刃在15-30度之间，切削一个切口或着几个。切割刀具的刀刃和边缘情况良好是特别重要的。1
46、0.2 CuttingGuide-Ifcutsaremademanually(asopposedtoamechanicalapparatus)asteelorotherhardmetalstraightedgeortemplatetoensurestraightcuts.切割指导：如果是手动切削钢制或其他金属直棱或模板要确保直线切割。10.3 Rule-Temperedsteelrulegraduatedin0.5mmformeasuringindividualcuts.规则：用刻度为0.5锻钢尺测量每个槽。10.4 Tape,asdescribedin5.3.胶带：见5.310.5 Rubb
47、erEraser,ontheendofapencil.铅笔末端的橡胶橡皮搽10.6 Illumination,asdescribedin5.5.照明描述见5.510.7 MagnifyingGlass-Anilluminatedmagnifiertobeusedwhilemakingindividualcutsandexaminingthetestarea.放大镜一一当切割单个的切口和在研究试验区时用一个照明放大器。11. TestSpecimens试样11.1 TestspecimensshallbeasdescribedinSection6.Itshouldbenoted,however,
48、thatmultitipcutters10providegoodresultsonlyontestareassufficientlyplanethatallcuttingedgescontactthesubstratetothesamedegree.Checkforflatnesswithastraightedgesuchasthatofthetemperedsteelrule(10.3).试样将在第6部分描述。应当记录，只有当试验区域足够平使切口在同一程度接触底材时，得到好的结果。12. ProCedUre程序12.1 Whererequiredorwhenagreedupon,subjectthespecimenstoapreliminarytestbeforeconductingthetapetest(seeNote3).Afterdryingortestingthecoating,conductthetapetestatroomtemperatureasdefinedinSpecificationD3924,unlessD3924standardtemperatureisrequiredoragreed.或在必要时达成协议,进行试验以前样本要经过初步测试。经过
